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The Journal of Organic Chemistry, ISSN 0022-3263, 10/2018, Volume 83, Issue 19, pp. 11577 - 11585
Oligonucleotides containing phosphorothioate (PS) linkages have recently demonstrated significant clinical utility. PS oligonucleotides are manufactured via a... 
REAGENT | 3-AMINO-1,2,4-DITHIAZOLE-5-THIONE | DNA | CHEMISTRY, ORGANIC | ANTISENSE OLIGONUCLEOTIDES | EFFICIENT | PHENYLACETYL DISULFIDE PADS
Journal Article
The Journal of Organic Chemistry, ISSN 0022-3263, 09/2013, Volume 78, Issue 18, pp. 9415 - 9423
Binaphthol-catalyzed asymmetric Petasis reactions of salicylaldehydes with dibutyl vinylboronates and secondary amines in the presence of 4 Å molecular sieves... 
BORONIC ACIDS | UNIFLORINE | ORGANOBORONIC ACIDS | CHIRAL BIPHENOLS | AMINES | ALLYLBORATION | ENONES | CHEMISTRY, ORGANIC | SALICYLALDEHYDES | ALDEHYDES | DERIVATIVES | Amines - chemistry | Vinyl Compounds - chemistry | Naphthols - chemistry | Boronic Acids - chemistry | Molecular Structure | Catalysis | Aldehydes - chemistry | Chirality | Research
Journal Article
ACS Symposium Series, ISSN 0097-6156, 2016, Volume 1239, pp. 69 - 100
Conference Proceeding
Organic Process Research & Development, ISSN 1083-6160, 03/2015, Volume 19, Issue 3, pp. 437 - 443
A two-step pharmaceutical manufacturing process was developed for the large-scale preparation of... 
NUCLEOSIDE | SURFACE-CONTROLLED DISSOLUTION | PARTICLES | CARBONATE | KINETICS | DIMETHYLFORMAMIDE | CHEMISTRY, ORGANIC | INHIBITORS | CHEMISTRY, APPLIED
Journal Article
Organic Process Research and Development, ISSN 1083-6160, 12/2014, Volume 19, Issue 8, pp. 935 - 948
A series of case histories from IQ consortium member companies are presented in order to exemplify many of the different elements of drug substance control... 
CHEMISTRY, ORGANIC | PALLADIUM REMOVAL | CATALYST | CHEMISTRY, APPLIED | SPECIATION
Journal Article
The Journal of Organic Chemistry, ISSN 0022-3263, 01/2012, Volume 77, Issue 2, pp. 1154 - 1160
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 05/2014, Volume 18, Issue 5, pp. 587 - 593
Designation and justification of active pharmaceutical ingredient starting material (API SM) is a standard part of the drug substance (DS) development and... 
CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED
Journal Article
Organic Process Research and Development, ISSN 1083-6160, 08/2015, Volume 19, Issue 8, pp. 915 - 924
Designation and justification of an Active Pharmaceutical Ingredient Starting Material (API SM) is an important aspect of the drug development and... 
CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 05/2014, Volume 18, Issue 5, pp. 594 - 600
Designation and justification of active pharmaceutical ingredient starting material (API SM) is a standard part of the drug development and commercialization... 
CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED
Journal Article
Organic Process Research and Development, ISSN 1083-6160, 08/2015, Volume 19, Issue 8, pp. 925 - 934
A number of strategies have been employed within the pharmaceutical industry in order to mitigate the risk of applying design space boundaries developed on the... 
CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED | VERIFICATION
Journal Article
Organic Process Research and Development, ISSN 1083-6160, 02/2012, Volume 16, Issue 2, pp. 232 - 239
Journal Article
Synthetic Communications, ISSN 0039-7911, 04/2007, Volume 37, Issue 8, pp. 1267 - 1272
Dimethyl bicyclo[2.2.2]octane-1,4-dicarboxylate (4), a key starting material for a novel adenosine A 1 receptor antagonist, was prepared in a one-pot reaction... 
stoichiometry | one-pot preparation | dimethyl bicyclo[2.2.2]octane-1,4-dicarboxylate
Journal Article
Journal of Labelled Compounds and Radiopharmaceuticals, ISSN 0362-4803, 03/2007, Volume 50, Issue 4, pp. 219 - 223
BG9928, a high affinity adenosine A1 antagonist, is currently in Phase II clinical trials for the treatment of congestive heart failure. A deuterium‐labeled... 
A1 antagonist | BG9928 | uracil | adenosine A1 receptor | bicyclo[2.2.2]octane | Bicyclo[2.2.2]octane | receptor | antagonist | Uracil | Adenosine A
Journal Article
Bioorganic & Medicinal Chemistry Letters, ISSN 0960-894X, 2005, Volume 15, Issue 3, pp. 511 - 515
A novel [1,2,4]triazolo[1,5-a]pyrazine core was synthesized and coupled with terminal acetylenes. The structure-activity relationship of the alkynes from this... 
A 2A antagonists | Parkinson’s disease | Triazolopyrazine | antagonists | Parkinson's disease
Journal Article
Journal of Organic Chemistry, ISSN 0022-3263, 1995, Volume 60, Issue 6, pp. 1713 - 1719
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 02/2012, Volume 16, Issue 2, pp. 232 - 239
The formation and fate of monomethyl sulfate (MMS) and dimethyl sulfate (DMS) were studied by proton NMR for a sulfuric acid catalyzed esterification reaction... 
CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED | ESTERS | WATER
Journal Article
Journal of Medicinal Chemistry, ISSN 0022-2623, 11/2006, Volume 49, Issue 24, pp. 7119 - 7131
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 02/1998, Volume 120, Issue 4, pp. 657 - 663
An extremely efficient method has been found for the catalytic asymmetric hydrogenation of conjugated α,γ-dienamide esters using the Et-DuPHOS-Rh catalyst... 
ROUTE | BIS(TRIARYL)PHOSPHINE | RHODIUM | ALPHA-(ACYLAMINO)ACRYLIC ACIDS | RADICAL CYCLIZATION | COMPLEXES | 2,2'-BIS(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHYL BINAP | DERIVATIVES | CHEMISTRY, MULTIDISCIPLINARY | ASYMMETRIC HOMOGENEOUS HYDROGENATION | STEREOSELECTIVE SYNTHESIS | Amino acids | Esters | Research | Catalysis | Hydrogenation | Analysis
Journal Article
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