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Tetrahedron, ISSN 0040-4020, 2006, Volume 62, Issue 19, pp. 4728 - 4732
The direct conversion of aryl halides to the corresponding phenols has been achieved using microwave heating. High-temperature or near-critical water is used... 
Phenols | Halides
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 06/2009, Volume 131, Issue 24, pp. 8578 - 8586
Journal Article
The Journal of Organic Chemistry, ISSN 0022-3263, 05/2008, Volume 73, Issue 10, pp. 3854 - 3858
We present here a strategy for the preparation of nonsymmetrically substituted stilbenes using a one-pot two-step double Heck strategy. First a protocol is... 
HALIDES | PALLADIUM | CATALYSIS | MECHANISM | PALLADACYCLES | CHEMISTRY | CHEMISTRY, ORGANIC | ARYL | Stereoisomerism | Stilbenes - chemical synthesis | Molecular Structure | Stilbenes - chemistry | Catalysis | Ethylenes - chemistry | Palladium - chemistry | Hydrocarbons, Halogenated - chemistry | Substitution reactions | Chemical properties | Analysis | Ethylene | Styrene
Journal Article
Journal of Medicinal Chemistry, ISSN 0022-2623, 09/2018, Volume 61, Issue 17, pp. 7525 - 7545
Past studies have shown that it has been difficult to discover and develop potent and selective κ opioid receptor antagonists, particularly compounds having... 
IN-VITRO | CHEMISTRY, MEDICINAL | SINGLE | PHARMACOKINETICS | ANALOGS | TOLERABILITY | RATS | SEEKING | ETHANOL | IDENTIFICATION | BRAIN
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 01/2010, Volume 14, Issue 1, pp. 205 - 214
A new batch microwave reactor has been evaluated in the context of palladium-mediated transformations, condensation reactions, nucleophilic aromatic... 
ASSISTED SYNTHESIS | SUZUKI | IRRADIATION | VESSEL | HEATING ELEMENTS | SOLVENT-FREE | PROMOTED REACTIONS | CHEMISTRY, ORGANIC | OPTIMIZATION | CHEMISTRY, APPLIED | INHIBITOR | APPARATUS
Journal Article
Synlett, ISSN 0936-5214, 7/2006, Volume 2006, Issue 11, pp. 1663 - 1666
Abstract The microwave-promoted hydroxycarbonylation of aryl iodides using reaction vessels pre-pressurized with CO is reported. Reactions are performed using... 
letter | Water | Microwave | Palladium | Catalysis | Carbonylations | ASSISTED ORGANIC-SYNTHESIS | AMINOCARBONYLATIONS | CATALYZED CARBONYLATION | INCREASING RATES | carbonylations | PALLADIUM COMPLEXES | CHEMISTRY, ORGANIC | catalysis | water | METHODOLOGY | COUPLING REACTIONS | ARYL HALIDES | CHEMISTRY | CHLORIDES | palladium | microwave
Journal Article
Tetrahedron Letters, ISSN 0040-4039, 2006, Volume 47, Issue 2, pp. 217 - 220
The Suzuki reaction in water using parts per million concentrations of palladium is reported using potassium trifluoroborates as alternatives to boronic acids... 
ORGANIC-SYNTHESIS | METHODOLOGY | CHEMISTRY | CHEMISTRY, ORGANIC | BOND FORMATION | SALTS | ALUMINA
Journal Article
Organic and Biomolecular Chemistry, ISSN 1477-0520, 2007, Volume 5, Issue 1, pp. 65 - 68
The microwave-promoted alkoxycarbonylation of aryl iodides using reaction vessels pre-pressurized with carbon monoxide is reported. Reactions are performed... 
ASSISTED ORGANIC-SYNTHESIS | HALIDES | AMINOCARBONYLATIONS | INCREASING RATES | PALLADIUM-CATALYZED CARBONYLATION | CHLORIDES | CHEMISTRY | CHEMISTRY, ORGANIC | BROMIDES | WATER
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 1/2008, Volume 12, Issue 1, pp. 41 - 57
In this report, we look at a range of classes of reaction involving microwave heating and show how different processing techniques can be used to address... 
ORGANIC-SYNTHESIS | SOLVENT-FREE | ASSISTED BECKMANN REARRANGEMENT | SOLID-PHASE SYNTHESIS | PRESSURIZED REACTION VESSELS | CHEMISTRY, ORGANIC | GASEOUS CARBON-MONOXIDE | DRY-MEDIA REACTOR | CHEMISTRY, APPLIED | HECK REACTION | DIHYDROPYRIDINE ESTER SYNTHESIS | METAL CATALYST CONCENTRATIONS
Journal Article
Journal of Medicinal Chemistry, ISSN 0022-2623, 09/2018, Volume 61, Issue 17, pp. 7546 - 7559
Animal pharmacological studies suggest that potent and selective κ opioid receptor antagonists have potential as pharmacotherapies targeting depression,... 
CHEMISTRY, MEDICINAL | PHARMACOKINETICS | CLONING | FUNCTIONAL EXPRESSION | TOLERABILITY | RATS | SEEKING | ETHANOL | IDENTIFICATION | BRAIN | DURATION
Journal Article
Synlett, ISSN 0936-5214, 8/2007, Volume 2007, Issue 13, pp. 2006 - 2010
Abstract Alkoxycarbonylation reactions using near-stoichio­metric quantities of carbon monoxide gas are presented. The reactions are performed using microwave... 
letter | Water | Microwave | Palladium | Catalysis | Carbonylations | HALIDES | CARBONYLATION | carbonylations | PRESSURIZED REACTION VESSELS | CHEMISTRY, ORGANIC | palladium | catalysis | GASEOUS CARBON-MONOXIDE | ARYL | water | microwave | PALLADIUM CATALYSTS
Journal Article
Journal of Chromatography A, ISSN 0021-9673, 2008, Volume 1211, Issue 1, pp. 49 - 54
Journal Article
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 05/2009, Volume 13, Issue 3, pp. 634 - 637
The ethoxycarbonylation of iodobenzene was performed on the 1 mol scale in batch mode using microwave heating. The reaction was performed using both an excess... 
AMINOCARBONYLATIONS | PALLADIUM-CATALYZED CARBONYLATION | PRESSURIZED REACTION VESSELS | PROMOTED REACTIONS | ARYL HALIDES | CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED | APPARATUS | PEAT | WATER
Journal Article
Journal Article
Organic Process Research & Development, ISSN 1083-6160, 11/2008, Volume 12, Issue 6, pp. 1078 - 1088
A range of synthetic transformations have been scaled up successfully using a sealed-vessel multimode microwave unit. These include metal-catalyzed couplings,... 
ASSISTED ORGANIC-SYNTHESIS | SUZUKI COUPLING REACTIONS | RAPID OPTIMIZATION | PRESSURIZED REACTION VESSELS | CHEMISTRY, ORGANIC | GASEOUS CARBON-MONOXIDE | CHEMISTRY, APPLIED | HISTONE DEACETYLASE INHIBITORS | CLAISEN REARRANGEMENT | METAL CATALYST CONCENTRATIONS | SITU RAMAN-SPECTROSCOPY | COUMARIN DERIVATIVES
Journal Article
Journal of Medicinal Chemistry, ISSN 0022-2623, 04/2014, Volume 57, Issue 7, pp. 3140 - 3147
N-substituted trans-3,4-dimethyl-4-(3-hydroxyphenyl)­piperidines (2a,b) are opioid receptor antagonists where the antagonist properties are not due to the type... 
Cricetinae | Piperidines - chemistry | Animals | Cricetulus | Magnetic Resonance Spectroscopy | Piperidines - pharmacology | Humans | Narcotic Antagonists - pharmacology | Structure-Activity Relationship | Radioligand Assay | Narcotic Antagonists - chemistry | CHO Cells
Journal Article
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