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Organic Letters, ISSN 1523-7060, 05/2015, Volume 17, Issue 10, pp. 2442 - 2445
Tris(2,2,2-trifluoroethyl)borate [B(OCH2CF3)3] was found to be a mild and general reagent for the formation of a variety of imines by condensation of amides or... 
Hydrocarbons, Fluorinated - chemistry | Molecular Structure | Imines - chemical synthesis | Borates - chemistry | Imines - chemistry
Journal Article
Journal of Labelled Compounds and Radiopharmaceuticals, ISSN 0362-4803, 08/2018, Volume 61, Issue 10, pp. 764 - 772
1‐(4‐Fluorophenyl)‐1H‐pyrazolo[3,4‐c]pyridine‐4‐carboxylic acid (2‐methanesulfonyl‐pyridin‐4‐ylmethyl)‐amide (1) and its analogs (2) and (3) are potent CCR1... 
radiosynthesis | tritium | carbon‐13 | carbon‐14 | CCR1 antagonists | carbon-14 | carbon-13 | RHEUMATOID-ARTHRITIS | CHEMISTRY, ANALYTICAL | CHEMISTRY, MEDICINAL | BIOCHEMICAL RESEARCH METHODS
Journal Article
Advanced Synthesis & Catalysis, ISSN 1615-4150, 01/2013, Volume 355, Issue 1, pp. 47 - 52
A mild and general procedure for reduction of primary, secondary, and tertiary amides using catalytic triruthenium dodecacarbonyl and... 
silanes | ruthenium | amides | reduction | SYSTEM | SELF-ENCAPSULATION | COMPLEX | SILANE REDUCTION | HYDROSILANES | CHEMISTRY, ORGANIC | CONVENIENT | CARBOXAMIDES | CHEMOSELECTIVE REDUCTION | CHIMIE ORGANIQUE | CATALYZED REDUCTION | CHEMISTRY, APPLIED | Amides | Amines | Ruthenium | Silane | Silanes | Reduction | Catalysts | Accessibility | Crystallization | Catalysis
Journal Article
Organic Letters, ISSN 1523-7060, 01/2011, Volume 13, Issue 1, pp. 118 - 121
A formal synthesis of berkelic acid is reported. The strategy employs the combination of a chiral exocyclic enol ether and an achiral isochromanone to afford... 
(-)-BERKELIC ACID | CYCLOADDITION | REAGENTS | LACTONES | NATURAL-PRODUCTS | O-QUINONE METHIDES | CHEMISTRY, ORGANIC | CARBONYL-COMPOUNDS | SPIROKETAL | CANCER | Molecular Structure | Cyclization | Oxidation-Reduction | Stereoisomerism | Spiro Compounds - chemical synthesis
Journal Article
Journal Article
Organic Letters, ISSN 1523-7060, 11/2015, Volume 17, Issue 22, pp. 5614 - 5617
A general, scalable, and highly diastereoselective aziridination of N-tert-butanesulfinyl ketimino esters is described. The methodology has been utilized to... 
Stereoisomerism | Aza Compounds - chemistry | Esters | Molecular Structure | Catalysis | Aziridines - chemistry | Aziridines - chemical synthesis
Journal Article
Tetrahedron Letters, ISSN 0040-4039, 04/2016, Volume 57, Issue 17, pp. 1903 - 1905
Triisopropyl borate effects the condensation of aldehydes with sulfinamides to give -sulfinyl imines. The reaction is amenable to 1°, 2°, and 3° alkyl... 
Imine | Borate | Condensation | Sulfinamide | KETONES | ASYMMETRIC-SYNTHESIS | AMINES | TERT-BUTANESULFINYL KETIMINES | CHEMISTRY, ORGANIC | ALDEHYDES | Aldehydes | Schiff bases | Borates | Filtration | Imines | Reagents | Tetrahedrons | Byproducts
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 11/2016, Volume 138, Issue 47, pp. 15473 - 15481
Journal Article
Green Chemistry, ISSN 1463-9262, 2017, Volume 19, Issue 6, pp. 1454 - 1461
A convergent, robust, and concise synthesis of a developmental CCR1 antagonist is described using continuous flow technology. In the first approach, following... 
Journal Article
GREEN CHEMISTRY, ISSN 1463-9262, 03/2017, Volume 19, Issue 6, pp. 1454 - 1461
Journal Article
Organic Letters, ISSN 1523-7060, 04/2008, Volume 10, Issue 7, pp. 1477 - 1480
A variety of chroman spiroketals are synthesized via inverse-demand [4 + 2] cycloaddition of enol ethers and ortho-quinone methides (o-QMs). Low temperature... 
CHEMISTRY, ORGANIC | ACID | RUBROMYCINS | NITRILES | COMPLEXES | Biological Products - chemical synthesis | Stereoisomerism | Spiro Compounds - chemical synthesis | Chromans - chemical synthesis | Ethers - chemistry | Indolequinones - chemistry | Molecular Structure | Furans - chemical synthesis
Journal Article
ISSN 1463-9262, 3/2017, Volume 19, Issue 6, pp. 1454 - 1461
A convergent, robust, and concise synthesis of a developmental CCR1 antagonist is described using continuous flow technology. In the first approach, following... 
Journal Article
Organic Letters, ISSN 1523-7060, 08/2006, Volume 8, Issue 16, pp. 3481 - 3483
(±)-Mitorubrinic acid, a member of the azaphilone family of natural products, has been constructed in 12 steps. Key aspects of the synthesis include... 
FUNGI | PENICILLIUM-FUNICULOSUM | AZAPHILONES | CHEMISTRY, ORGANIC | CYCLOISOMERIZATION | MITORUBRIN | METABOLITE | DEAROMATIZATION
Journal Article
Journal Article
Organic Letters, ISSN 1523-7060, 05/2009, Volume 11, Issue 9, pp. 1955 - 1958
Chemoselective additions of organometallic reagents to 3-benzyloxy-1,2-o-quinone are described. Various nucleophiles are shown to undergo selective... 
OXIDATION | ORTHO-QUINONES | CYCLOADDITION | DIELS-ALDER REACTIONS | ENANTIOSELECTIVE SYNTHESIS | O-BENZOQUINONES | REDUCTION | LEWIS-ACID | ALLYLATION | CHEMISTRY, ORGANIC | DERIVATIVES
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 04/2013, Volume 135, Issue 15, pp. 5565 - 5568
Journal Article
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