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Industrial & Engineering Chemistry Research, ISSN 0888-5885, 12/2016, Volume 55, Issue 50, pp. 12786 - 12794
In this work the general Ψ number criterion for the safe operation of semibatch runaway reactions has been applied to the optimization of a nitration process... 
ENGINEERING, CHEMICAL | REACTORS | LIMITS | AROMATIC NITRATIONS | ARBITRARY REACTION ORDER | OPERATION | MIXED ACID | SYSTEMS | CRITERION | LIQUID-LIQUID REACTIONS | REACTION REGIME
Journal Article
Industrial & Engineering Chemistry Research, ISSN 0888-5885, 02/2016, Volume 55, Issue 4, pp. 925 - 933
In this work, a simple and general method has been developed that, on the basis of an easy-to-measure quantity referred to as the Ψ number, allows for ongoing... 
ENGINEERING, CHEMICAL | LIMITS | LIQUID SEMIBATCH REACTORS | ARBITRARY REACTION ORDER
Journal Article
Industrial & Engineering Chemistry Research, ISSN 0888-5885, 07/2017, Volume 56, Issue 26, pp. 7434 - 7444
A number of potential runaway reaction systems of the fine chemical industry (e.g., polymerization processes) undergo significant changes of their physical... 
DIAGRAMS | ENGINEERING, CHEMICAL | CHEMICAL REACTORS | THERMALLY SAFE OPERATION | PRECIPITATION POLYMERIZATION | GENERAL CRITERION | RUNAWAY PREVENTION | ACRYLIC-ACID | DIVERGENCE CRITERION | LIQUID-LIQUID REACTIONS | NITRATION
Journal Article
Chemical engineering science, ISSN 0009-2509, 2019, Volume 203, pp. 173 - 185
•Different approaches for modelling DR-PSA units are presented and compared.•The approaches are tested for both complete and non-complete separation cases.•The... 
Dual-reflux | Finite volume method | Gas separation | Pressure swing adsorption | Cyclic adsorption process | Finite difference method | OPTIMAL-DESIGN | CO2 | PSA PROCESS | SIMULATION | ENGINEERING, CHEMICAL | EQUILIBRIUM-THEORY ANALYSIS | CYCLES | GAS | OPTIMIZATION | SEPARATION | UNITS
Journal Article
Chemical engineering journal (Lausanne, Switzerland : 1996), ISSN 1385-8947, 2019, Volume 373, pp. 792 - 802
[Display omitted] •A procedure for transforming a non-isothermal SBR process into a tubular reactor one is proposed.•The tubular reactor involves both a... 
Process Intensification | Semi-batch to continuous | Kinetics-free | Tubular reactor | Flow chemistry | ENGINEERING, CHEMICAL | ENGINEERING, ENVIRONMENTAL | COPOLYMERIZATION | SEMIBATCH | Case studies | Chemical reaction, Rate of
Journal Article
Industrial & engineering chemistry research, ISSN 0888-5885, 04/2019, Volume 58, Issue 16, pp. 6644 - 6652
In the frame of dual-reflux pressure swing adsorption processes, design strategies applicable to the complete separation of binary gas mixtures are available... 
ENGINEERING, CHEMICAL | CYCLES | CO2 | GAS | OPTIMIZATION | SIMULATION | CAPTURE | PSA
Journal Article
Industrial & engineering chemistry research, ISSN 0888-5885, 02/2019, Volume 58, Issue 6, pp. 2181 - 2194
Whenever the productivity of an indirectly cooled, isoperibolic semibatch reactor (SBR) must be enhanced by keeping the reaction temperature nearly constant,... 
ENGINEERING, CHEMICAL | THERMALLY SAFE OPERATION | NITRATION
Journal Article
Chemical engineering journal (Lausanne, Switzerland : 1996), ISSN 1385-8947, 2018, Volume 354, pp. 1007 - 1017
•A methodology for transforming a SBR process into a tubular reactor one is proposed.•The tubular reactor involves a properly defined continuous side feed.•The... 
Semi-batch to continuous | Process intensification | Kinetics-free | Tubular reactor | EMULSION POLYMERIZATION | STYRENE | AQUEOUS-SOLUTION | ENGINEERING, CHEMICAL | ENGINEERING, ENVIRONMENTAL | HEAT-EXCHANGERS | SYSTEMS | SAFE OPTIMIZATION | COPOLYMERIZATION | Case studies | Fine chemicals | Industrial productivity
Journal Article
Industrial & Engineering Chemistry Research, ISSN 0888-5885, 10/2017, Volume 56, Issue 39, pp. 11075 - 11087
A number of exothermic semibatch (SB) processes of the fine chemical industry may undergo selectivity drops because of the triggering of consecutive... 
ENGINEERING, CHEMICAL | DECOMPOSITION | REACTORS | MAXIMUM TEMPERATURE | OPERATION | RUNAWAY
Journal Article
Journal of Loss Prevention in the Process Industries, ISSN 0950-4230, 11/2016, Volume 44, pp. 311 - 322
Combustible dust explosions are among the most serious criticalities affecting a broad number of industries around the world. According to a Chemical Safety... 
Explosion severity | Explosion parameters estimation | Combustible dust explosion | Deflagration index
Journal Article
Chemical Engineering Science, ISSN 0009-2509, 08/2018, Volume 186, pp. 219 - 227
[Display omitted] •SBRR allows increasing process selectivity and plant productivity with respect to SBR.•SBRR plant configuration can be easily assembled in... 
Semibatch Reactor (SBR) | Semibatch Recycle Reactor (SBRR) | Selectivity | Safety | Polyamines | Multipurpose processes | ENGINEERING, CHEMICAL | Production processes
Journal Article
Chemical Engineering Science, ISSN 0009-2509, 09/2015, Volume 134, pp. 708 - 720
A number of reaction processes of the fine chemical and pharma industry undergo selectivity losses, since the target product (often a low volatility compound)... 
Semibatch recycle reactor (SBRR) | Ethylene glycol | Selectivity | Ethylene oxide | Kinetics | Process control | ENGINEERING, CHEMICAL | LIQUID SEMIBATCH REACTORS | THERMALLY SAFE OPERATION | DISTILLATION PROCESSES
Journal Article
Industrial & Engineering Chemistry Research, ISSN 0888-5885, 02/2018, Volume 57, Issue 6, pp. 1980 - 1990
In the fine chemical industry, new production processes are often implemented in multipurpose existing plants with minimum adaptation investments. When the new... 
ENGINEERING, CHEMICAL | AROMATIC NITRATIONS | LIQUID SEMIBATCH REACTORS | THERMALLY SAFE OPERATION | MIXED ACID | POLYMERIZATION | OPTIMIZATION
Journal Article
Industrial & engineering chemistry research, ISSN 0888-5885, 01/2019, Volume 58, Issue 1, pp. 350 - 365
Binary gas mixtures can be completely separated via dual-reflux pressure swing adsorption (DR-PSA) process, where pressure of the column to which the feed gas... 
ENGINEERING, CHEMICAL | RECOVERY | OPTIMAL-DESIGN | CO2 | PSA PROCESS | OPTIMIZATION | SEPARATION | SIMULTANEOUS REMOVAL | SIMULATION | CAPTURE | UNITS
Journal Article
Journal of Loss Prevention in the Process Industries, ISSN 0950-4230, 03/2018, Volume 52, pp. 93 - 98
Even in recent years, several major industrial accidents have involved dust explosions, clearly showing the necessity of mitigating the hazard related to the... 
Organic dust explosion | Explosion severity | Experimental data | Kinetic-free model | Deflagration index | Modeling
Journal Article
Chemical Engineering Science, ISSN 0009-2509, 01/2015, Volume 122, pp. 34 - 52
Journal Article
Journal Article
Chemical engineering journal (Lausanne, Switzerland : 1996), ISSN 1385-8947, 2017, Volume 311, pp. 385 - 406
•An optimal design strategy is presented for the process configuration DR-PL-A.•Key parameters needed to establish complete separation at CSS are... 
Dual-reflux | PSA design | Gas separation | Equilibrium theory | Pressure swing adsorption | Cyclic adsorption process | CO2 | PSA PROCESS | AIR | SIMULTANEOUS REMOVAL | SIMULATION | ENGINEERING, CHEMICAL | RECOVERY | ENGINEERING, ENVIRONMENTAL | CYCLES | ENRICHMENT | SEPARATION | Adsorption | Analysis
Journal Article
Environmental Science and Pollution Research, ISSN 0944-1344, 3/2014, Volume 21, Issue 6, pp. 4320 - 4330
Journal Article
Journal of loss prevention in the process industries, ISSN 0950-4230, 2018, Volume 55, pp. 289 - 302
A great variety of processes of both fine chemical and pharmaceutical industries are commonly carried out in semibatch reactors (SBRs). Most of such syntheses... 
Runaway reactions | Nitration reactions | Series of continuous reactors | Process intensification | Shift to a continuous process | LIMITS | CONTROLLED CSTR | COOLED SEMIBATCH REACTOR | SENSITIVITY | CHAOTIC BEHAVIOR | IDENTIFICATION | ENGINEERING, CHEMICAL | CHEMICAL REACTORS | OPERATION | CRITERION | NITRATION | Case studies | Nitration | Sulfonamides | Analysis | Fine chemicals
Journal Article
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