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Journal of the American Chemical Society, ISSN 0002-7863, 10/2015, Volume 137, Issue 40, pp. 12808 - 12814
A new bifunctional pincer ligand framework bearing pendent proton-responsive hydroxyl groups was prepared and metalated with Ru­(II) and subsequently isolated... 
H BOND ACTIVATION | REDUCTION | HYDROGEN-BOND | 2ND COORDINATION SPHERE | CARBONYL-COMPOUNDS | PRIMARY AMINES | SIGMA-BONDS | LIGAND | CHEMISTRY, MULTIDISCIPLINARY | HETEROLYTIC CLEAVAGE | HYDRIDE COMPLEXES | Protons | Crystallography, X-Ray | Catalysis | Boron - chemistry | Ruthenium - chemistry | Nitriles - chemistry | Hydroboration | Ruthenium | Ketones | Nitriles | Research | Chemical properties
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 10/2016, Volume 138, Issue 41, pp. 13489 - 13492
We present the direct and stereoretentive deuteration of primary amines using Ru-bMepi (bMepi = 1,3-(6′-methyl-2′-pyridyl­imino)­isoindolate) complexes and... 
DEHYDROGENATION | MECHANISM | ALCOHOL | COMPLEXES | RUTHENIUM | RACEMIZATION | EXCHANGE | CHEMISTRY, MULTIDISCIPLINARY | DYNAMIC KINETIC RESOLUTION | DEUTERIUM | DISCOVERY | Ligands | Amines | Ruthenium | Chemical properties | Carbon compounds | Analysis
Journal Article
Chemical Communications, ISSN 1359-7345, 01/2013, Volume 49, Issue 4, pp. 400 - 402
The ligand 6,6'-dihydroxy terpyridine (dhtp) is presented as a bifunctional ligand capable of directing proton transfer events with metal-coordinated... 
SYSTEM | OXIDATION | ALCOHOLS | ASYMMETRIC TRANSFER HYDROGENATION | DEHYDROGENATION | CRYSTAL-STRUCTURE | AQUEOUS-MEDIA | H-2 ACTIVATION | IRON COMPLEX | CHEMISTRY, MULTIDISCIPLINARY | WATER | Utilities | Catalysts | Ketones | Chlorides | Ligands | Catalysis | Hydrogenation | Hydroxyl groups
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 07/2017, Volume 139, Issue 29, pp. 9811 - 9814
We present a strategy to rationally prepare CF3 – transfer reagents at ambient temperature from HCF3. We demonstrate that a highly reactive CF3 – adduct can be... 
NUCLEOPHILIC TRIFLUOROMETHYLATION | CATALYSIS | HYDROGENATION | REDUCTION | EXCHANGE | CHEMISTRY, MULTIDISCIPLINARY | HYDRIDE | Usage | Halides | Research | Chemical properties | Methylation | Nucleophiles | Electrophiles | Carbon compounds
Journal Article
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, ISSN 0002-7863, 04/2017, Volume 139, Issue 16, pp. 5952 - 5956
We present a systematic investigation of the structural and electronic changes that occur in an Fe(0)-N-2 unit (Fe(depe)(2)(N-2); depe =... 
NITROGEN-FIXATION | CATALYTIC-REDUCTION | AMMONIA | ACTIVE-SITE | MOLYBDENUM | COORDINATED DINITROGEN | DINITROGEN COMPLEXES | LIGAND | PHOSPHINE COMPLEXES | BINDING | CHEMISTRY, MULTIDISCIPLINARY
Journal Article
Angewandte Chemie International Edition, ISSN 1433-7851, 02/2016, Volume 55, Issue 9, pp. 3101 - 3105
Journal Article
Chemical Communications, ISSN 1359-7345, 2017, Volume 53, Issue 14, pp. 2287 - 2289
Modification of the classic terpyridine pincer ligand with pendent NHR (R = mesityl) groups provides enhanced activity and stability in Ru-catalyzed... 
FUNCTIONAL BIPYRIDONATE LIGAND | OH GROUPS | IRIDIUM COMPLEX BEARING | DESIGN | DEHYDROGENATION | TRANSFER HYDROGENATION | PINCER-TYPE COMPLEXES | ACID SALTS | CHEMISTRY, MULTIDISCIPLINARY | RUTHENIUM CATALYST | WATER
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 12/2017, Volume 139, Issue 50, pp. 18194 - 18197
Incorporation of two 9-borabicyclo[3.3.1]­nonyl substituents within the secondary coordination sphere of a pincer-based Fe­(II) complex provides Lewis acidic... 
NITROGEN-FIXATION | TERMINAL NH2 GROUPS | COMPLEX | ACTIVATION | HYDROGENATION | AMMONIA | CARBON-MONOXIDE | COORDINATION | COOPERATIVITY | LIGAND | CHEMISTRY, MULTIDISCIPLINARY | Lewis Acids - chemistry | Hydrazines - chemistry | Nitrogen - chemistry | Oxidation-Reduction | Iron - chemistry | Molecular Structure | Coordination Complexes - chemistry
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 08/2016, Volume 138, Issue 33, pp. 10378 - 10381
A new series of bifunctional Ru complexes with pendent Lewis acidic boranes were prepared by late-stage modification of an active hydrogen-transfer catalyst.... 
ACTIVATION | HYDROBORATION | TEMPERATURE | BIFUNCTIONAL CATALYSTS | B-C BOND | COMPLEXES | COORDINATION | PROTON | BORANE | CHEMISTRY, MULTIDISCIPLINARY | RHODIUM(I)
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 11/2013, Volume 135, Issue 44, pp. 16352 - 16355
Journal Article
Chemical Communications, ISSN 1359-7345, 2016, Volume 52, Issue 14, pp. 2901 - 2904
An amide-derived N,N,N-Ru(II) complex catalyzes the conversion of EtOH to 1-BuOH with high activity. Conversion to alcohol upgraded products exceeds 250... 
ALCOHOLS | HYDROGEN | DECARBONYLATION | DEHYDROGENATION | PERSPECTIVE | N-BUTANOL | ADVANCED BIOFUEL | METAL | ACCEPTORLESS | SELECTIVITY | CHEMISTRY, MULTIDISCIPLINARY
Journal Article
Chemical science, ISSN 2041-6520, 06/2015, Volume 6, Issue 6, pp. 3373 - 3377
Nitrite reduction by a copper complex featuring a proton-responsive tripodal ligand is demonstrated. Gaseous nitric oxide was confirmed as the sole NO... 
Journal Article
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, ISSN 0002-7863, 08/2018, Volume 140, Issue 32, pp. 10075 - 10079
Six directed hydrogen bonding (H-bonding) interactions allow for the reversible capture and reduction of dioxygen to a trans-1,2-peroxo within a tripodal... 
DIOXYGEN ACTIVATION | REDUCTION | AZIDE COMPLEXES | REACTIVITY | COORDINATION | COPPER | LEWIS-ACIDS | LIGAND | DERIVATIVES | CHEMISTRY, MULTIDISCIPLINARY | PEROXIDE | Heme - chemistry | Hydrogen Bonding | Oxygen - chemistry | Peroxides - chemistry | Models, Molecular | Molecular Structure | Zinc
Journal Article
Inorganic Chemistry, ISSN 0020-1669, 01/2019, Volume 58, Issue 2, pp. 1147 - 1154
An iron complex bearing a pyridine(dicarbene) pincer was designed to probe the requirements of Lewis acid enabled N2H4 capture and subsequent N-N bond... 
NITROGENASE | N-2 | REDUCTION | HYDROGEN-BOND | PINCER DICARBENE COMPLEXES | REACTIVITY | DINITROGEN | MECHANISMS | LIGAND | CATALYSTS | CHEMISTRY, INORGANIC & NUCLEAR
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 08/2018, Volume 140, Issue 30, pp. 9404 - 9408
The difluoromethyl group (R–CF2H) imparts desirable pharmacokinetic properties to drug molecules and is commonly targeted as a terminal functional group that... 
ORGANOZINC REAGENTS | TRI | CHEMISTRY, MULTIDISCIPLINARY | FLUORIDE
Journal Article
Chemical communications (Cambridge, England), ISSN 1359-7345, 03/2015, Volume 51, Issue 25, pp. 5490 - 5492
Chemical reduction of a tripodal Cu(II)-F complex containing pendent hydroxyl groups results in the partial dissociation of a F(-) ligand from Cu. The... 
Journal Article
Chemical Communications, ISSN 1359-7345, 2018, Volume 54, Issue 8, pp. 892 - 895
A series of copper complexes bearing new 6-substituted tris(2-pyridyl-methyl)amine ligands (L-R) appended with NH(p-R-C6H4) groups (R = H, CF3, OMe) were... 
COPPER-DIOXYGEN COMPLEXES | D-BETA-M | ACTIVATION | ELECTRON-TRANSFER | SPECTROSCOPY | REDUCTION | REACTIVITY | ADDUCTS | MODEL | LIGAND SUBSTITUENT | CHEMISTRY, MULTIDISCIPLINARY
Journal Article
Angewandte Chemie International Edition, ISSN 1433-7851, 01/2018, Volume 57, Issue 5, pp. 1381 - 1385
Journal Article
CHEMICAL COMMUNICATIONS, ISSN 1359-7345, 05/2019, Volume 55, Issue 35, pp. 5119 - 5122
Difluoromethane (CF2H2) is an ecologically-friendly refrigerant which holds promise as a source of CF2H-. However, the weak acidity (pK(a) = 35-41) and low... 
REAGENTS | ACIDITIES | CHEMISTRY, MULTIDISCIPLINARY | TRIFLUOROMETHYLATION
Journal Article
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