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Organic Letters, ISSN 1523-7060, 09/2013, Volume 15, Issue 17, pp. 4520 - 4523
A new iterative one-pot sequential method for the solution-phase synthesis of oligosaccharides has been devised on the basis of the electrochemical oxidation... 
CHEMISTRY, ORGANIC | BETA-MANNOPYRANOSIDES | GENERATION | GLYCOSYLATION | OLIGOGLUCOSAMINES | POLYSACCHARIDE
Journal Article
Carbohydrate Research, ISSN 0008-6215, 07/2019, Volume 480, pp. 7 - 11
Direct 6-thiophosphorylation of mannopyranoside gave both the wanted - as well as the undesired -phosphates. This required sequential protecting group... 
Mannopyranoside 6-thiophosphate | Mannopyranoside 6-phosphate | Affinity ligands | 6-Deoxy-6-thio-mannopyranoside 6-phosphate | (Thio)Phosphorylation | 6-PHOSPHATE | BIOCHEMISTRY & MOLECULAR BIOLOGY | CHEMISTRY, ORGANIC | CHEMISTRY, APPLIED | Phosphates | Sugars | Chromatography | Monosaccharides
Journal Article
NATURE CHEMISTRY, ISSN 1755-4330, 08/2012, Volume 4, Issue 8, pp. 663 - 667
Although arguably the most important reaction in glycoscience, chemical glycosylations are among the least well understood of organic chemical reactions,... 
C-MANNOPYRANOSIDES | NATURAL-ABUNDANCE | DENSITY | CHEMISTRY | REACTIVITY | IONS | DONORS | EXCHANGE | CHEMISTRY, MULTIDISCIPLINARY | GLYCOBIOLOGY | CATIONS
Journal Article
by Zhu, YG and Yu, B
CHEMISTRY-A EUROPEAN JOURNAL, ISSN 0947-6539, 06/2015, Volume 21, Issue 24, pp. 8771 - 8780
Journal Article
Organic Letters, ISSN 1523-7060, 02/2014, Volume 16, Issue 3, pp. 716 - 719
O-Picoloyl groups at remote positions can mediate the course of glycosylation reactions by providing high facial selectivity for the H-bond-mediated attack of... 
MANNOPYRANOSIDES | STEREOSELECTIVITY | CHEMISTRY | GLYCOCHEMISTRY | CHEMISTRY, ORGANIC | CHEMOSELECTIVE OLIGOSACCHARIDE SYNTHESIS | MANNOSIDES | PROTECTING GROUPS | CHEMICAL GLYCOSYLATION | PRINCIPLES | Glycosylation | Molecular Structure | Hydrogen Bonding | Mannosides - chemistry | Stereoisomerism | Hydrogen - chemistry
Journal Article
ORGANIC LETTERS, ISSN 1523-7060, 02/2014, Volume 16, Issue 4, pp. 1116 - 1119
Mannosylations using the new conformationally restricted donor phenyl 2,3-di-O-benzyl-4,6-O-(di-tert-butylsilylene)-1-thio-alpha-D-mannopyranoside (6) have... 
ELECTROSTATIC INTERACTIONS | MANNOPYRANOSIDES | THIOGLYCOSIDES | DIETHYL PHOSPHITE | GLYCOSYL DONORS | REACTIVITY | CHEMISTRY, ORGANIC | CHEMICAL-SYNTHESIS | PROTECTING GROUPS | STEREOSELECTIVE-SYNTHESIS | OXOCARBENIUM IONS
Journal Article
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, ISSN 0002-7863, 10/2019, Volume 141, Issue 42, pp. 16743 - 16754
Here we demonstrate that highly beta-selective glycosylation reactions can be achieved when the electronics of a sulfonyl chloride activator and the reactivity... 
ALCOHOLS | TRANSITION-STATE STRUCTURE | ALPHA-GLUCOPYRANOSYL | HYDROLYSIS | BETA-D-MANNOPYRANOSIDES | MECHANISMS | STEREOSELECTIVE-SYNTHESIS | PROTECTING GROUPS | GLYCOSIDATION | CHEMISTRY, MULTIDISCIPLINARY | ANHYDRIDE
Journal Article
Chemical Science, ISSN 2041-6520, 2017, Volume 8, Issue 3, pp. 1867 - 1875
A set of model nucleophiles of gradually changing nucleophilicity is used to probe the glycosylation reaction mechanism. Glycosylations of ethanol-based... 
MANNURONIC ACID-ESTERS | BETA-MANNOPYRANOSIDES | SOLID-PHASE SYNTHESIS | POT OLIGOSACCHARIDE SYNTHESIS | C-GLYCOSYLATION | PSEUDOAXIAL CONFORMERS | CATION CLOCK REACTIONS | STEREOSELECTIVE-SYNTHESIS | CHEMICAL GLYCOSYLATION | OXOCARBENIUM IONS | CHEMISTRY, MULTIDISCIPLINARY
Journal Article
CHEMICAL COMMUNICATIONS, ISSN 1359-7345, 03/2017, Volume 53, Issue 21, pp. 3018 - 3021
Regio- and stereoselective b-mannosylations using 1,2-anhydromannose and diol sugar acceptors in the presence of a boronic acid catalyst proceeded smoothly to... 
TRANSIENT MASKING | SIDE-CHAINS | HYDROXY-GROUPS | REGIOSELECTIVE GLYCOSYLATION | SELECTIVE MANNOSYLATION | D-MANNOPYRANOSIDES | DISACCHARIDES | ANOMERIC O-ALKYLATION | GLYCOSIDIC LINKAGES | CHEMISTRY, MULTIDISCIPLINARY | STANNYLENE ACTIVATION
Journal Article
Chemistry – A European Journal, ISSN 0947-6539, 06/2015, Volume 21, Issue 24, pp. 8771 - 8780
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 01/2016, Volume 138, Issue 1, pp. 444 - 456
Journal Article
The Journal of Organic Chemistry, ISSN 0022-3263, 07/2018, Volume 83, Issue 13, pp. 7180 - 7205
The commercial macrolide antibiotic fidaxomicin was synthesized in a highly convergent manner. Salient features of this synthesis include a β-selective... 
CLOSTRIDIUM-DIFFICILE INFECTION | BETA-MANNOPYRANOSIDES | NATURAL-PRODUCT | CO-IDENTITY | SILYL N,O-ACETAL | CONVENIENT PREPARATION | BIOLOGICAL-ACTIVITY | MUKAIYAMA ALDOL REACTION | CHEMISTRY, ORGANIC | MACROLIDE ANTIBIOTICS | RNA-POLYMERASE
Journal Article
Journal Article
Journal of the American Chemical Society, ISSN 0002-7863, 09/2017, Volume 139, Issue 36, pp. 12736 - 12744
Journal Article
Organic Letters, ISSN 1523-7060, 08/2013, Volume 15, Issue 16, pp. 4170 - 4173
N-Sulfonyl imidazoles activate 2-deoxy-sugar hemiacetals for glycosylation presumably by converting them into glycosyl sulfonates in situ. By matching the... 
DE-NOVO SYNTHESIS | D-MANNOPYRANOSIDES | LANDOMYCIN-A | HEXASACCHARIDE FRAGMENT | DIRECT CONSTRUCTION | CHEMISTRY, ORGANIC | GANGLIOSIDE ANALOGS | HIGHLY STEREOSELECTIVE-SYNTHESIS | GLYCOSIDATION | GLYCAL PRECURSORS | 2-DEOXY-BETA-GLYCOSIDES
Journal Article
Chemical Science, ISSN 2041-6520, 02/2017, Volume 8, Issue 3, pp. 1867 - 1875
A set of model nucleophiles of gradually changing nucleophilicity is used to probe the glycosylation reaction mechanism. Glycosylations of ethanol-based... 
Stereoselectivity | Ethyl alcohol | Tools | Mannose | Robustness | Nucleophiles | Reaction mechanisms | Condensation
Journal Article
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