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乳业科学与技术, ISSN 1671-5187, 2015, Volume 38, Issue 3, pp. 34 - 38
R153.1; 2013年1月,新西兰牛乳及乳制品中双氰胺的检出,引起了全世界广泛的关注.因此,乳制品中双氰胺的检测方法成为了关注的热点问题.本文主要综述了乳及乳制品中双氰胺的高效液相色谱-串联质谱(high performance liquid chromatography-tandem mass... 
Journal Article
Bunseki kagaku, ISSN 0525-1931, 2018, Volume 67, Issue 5, pp. 249 - 279
Journal Article
昭和学士会雑誌, ISSN 2187-719X, 2016, Volume 76, Issue 3, pp. 369 - 381
カルバペネム系抗菌薬は殺菌性に優れ,かつ幅広い抗菌スペクトルを有し,敗血症等の重症難治性感染症の治療薬として広く使用されている.さらに,カルバペネム系抗菌薬は時間依存的な抗菌効果を示す.薬物動態(pharmacokinetics: PK)と薬力学(pharmacodynamics:... 
親水性相互作用液体クロマトグラフィー(HILIC) | UK-Aminoカラム | カルバペネム系抗菌薬 | タンデム質量分析(MS/MS) | 血漿
Journal Article
Biological and Pharmaceutical Bulletin, ISSN 0918-6158, 2018, Volume 41, Issue 4, pp. 597 - 603
Unusual bile acids (1β-hydroxylated bile acids), particularly 1β-hydroxyl-cholic acid (CA-1β-ol) and 1β-hydroxyl-chenodeoxycholic acid (CDCA-1β-ol), have been... 
Journal Article
Biological and Pharmaceutical Bulletin, ISSN 0918-6158, 2015, Volume 38, Issue 10, pp. 1518 - 1528
Coptisine (COP), a protoberberine alkaloid (PBA) from Chinese medicinal plants (such as family Berberidaceae), may be useful for improving central nervous... 
Journal Article
承德医学院学报, ISSN 1004-6879, 2015, Volume 32, Issue 5, pp. 425 - 427
R969.1 
Journal Article
by 袁娟娟 and 刘逊
Shanxi Zhong yi, ISSN 1000-7369, 2017, Volume 38, Issue 6, pp. 810 - 816
R684.3; 目的:探讨穿山甲炮制增效的机理.方法:采用TOF MS-IDA-MS/MS对穿山甲炮制前后成分变化进行研究,Waters C18色谱柱(2.1 mm×150 mm,1.7 μm);柱温40℃.流动相为0 min,乙腈-水(5∶95),30min乙腈-水(95∶5);体积流量0.4... 
Journal Article
云南化工, ISSN 1004-275X, 2017, Volume 44, Issue 5, pp. 39 - 43
TS42%O657.33;... 
Journal Article
by 陈林 and 温家欣 and 刘潇潇 and 雷毅 and 张荣
Zhong cheng yao, ISSN 1001-1528, 2017, Volume 39, Issue 3, pp. 556 - 560
R284.1; 目的 通过HPLC结合LC-MS/MS法快速检测穿山甲Manis Squama中掺加的12种黄色色素(柠檬黄、日落黄、酸性橙10、栀子黄、碱性嫩黄O、碱性橙21、碱性橙2、酸性橙2、皂黄、碱性橙22、酸性嫩黄G、奶油黄).方法 穿山甲70%甲醇提取液的HPLC分析采用Agilent Poroshell... 
Journal Article
by 杨梅 and 孙思 and 王安波 and 汪俭 and 刘文锋
Guizhou nong ye ke xue, ISSN 1001-3601, 2017, Volume 45, Issue 6, pp. 128 - 132
S859; 为家禽水产品中的氯霉素残留快速检测提供参考,以氯霉素-D5为内标,用乙酸乙酯提取样品氯霉素残留、正己烷进行脱脂净化、UPLC-MS/MS方法进行氯霉素残留含量检测.结果表明:在氯霉素浓度为0.2~10 ng/mL时,基质标准曲线的方程为Y=0.816 397X-0.038 239,R2 =0.998... 
Journal Article
中国临床药理学杂志, ISSN 1001-6821, 2017, Volume 33, Issue 19, pp. 1949 - 1953
R28; 目的 建立超高效液相色谱串联三重四级杆质谱(UPLC-MS/MS)同时测定积雪草中7种有效成分(积雪草苷B、羟基积雪草苷、积雪草苷、羟基积雪草酸、积雪草酸、槲皮素和山柰酚)的含量.方法 色谱柱:ACQUITYBEH C1s(2.1mm×100 mm,1.7 μm),流动相:乙腈-5... 
Journal Article
农药科学与管理, ISSN 1002-5480, 2017, Volume 38, Issue 3, pp. 45 - 48
S482.3%S481+.8; 系统研究克百威在蔬菜水果中的残留量,促进安全生产.采用乙腈提取,饱和氯化钠盐析后离心,上清液加少许PSA净化后过0.22μm滤膜,LC-MS/MS测定.该分析方法的添加回收率在86.2% ~... 
Journal Article
Chemical and Pharmaceutical Bulletin, ISSN 0009-2363, 2019, Volume 67, Issue 10, pp. 1104 - 1115
Licorice is one of the ancient and most frequently applied herbs for its diverse phytochemicals. At present, wild resources of licorice have rapidly declined... 
Journal Article
Fen xi ce shi xue bao, ISSN 1004-4957, 2017, Volume 36, Issue 8, pp. 975 - 979
O657.7%O657.63;... 
Journal Article
Biological and Pharmaceutical Bulletin, ISSN 0918-6158, 2014, Volume 37, Issue 1, pp. 18 - 25
A "cocktail" approach, which involves simultaneous administration of multiple CYP-specific probes, concurrently detects the activity of multiple CYP enzymes.... 
Journal Article
Journal of Pesticide Science, ISSN 1348-589X, 2019, Volume 44, Issue 3/4, pp. 186 - 191
A micro liquid-liquid extraction has been applied to sample preparation in the current authorized method for clopyralid in compost. The method rendered matrix... 
Journal Article
质谱学报, ISSN 1004-2997, 2017, Volume 38, Issue 2, pp. 248 - 255
O657.6;... 
Journal Article
Journal of the Mass Spectrometry Society of Japan, ISSN 1340-8097, 2014, Volume 62, Issue 5, pp. 61 - 64
IUPAC (International Union of Pure and Applied Chemistry) recommends that a hyphen, or, alternatively, a slash, should be used to indicate a combination of two... 
LC/MS | GC-MS | LC-MS | MS/MS | GC/MS
Journal Article
吉林中医药, ISSN 1003-5699, 2018, Volume 38, Issue 3, pp. 328 - 330
R284; 目的 通过固相萃取-电喷雾串联质谱(SPE-ESI-MS/MS)法快速分析血塞通中三七总皂苷成分.方法 采用Agilent SampliQ C18固相萃取柱对血塞通中三七总皂苷成分进行纯化和分离,通过ESI-MS/MS分析鉴定其皂苷类成分.结果... 
Journal Article
职业卫生与病伤, ISSN 1006-172X, 2016, Volume 31, Issue 3, pp. 183 - 185
R313; 目的 建立GC-MS-MS方法快速检测中毒样品中的克百威,及时应对突发性克百威中毒事件.方法 液体或半固体样品加无水硫酸钠吸水后,加乙酸乙酯萃取;固体样品和血液样品直接加乙酸乙酯萃取;萃取液氮吹后,正己烷定容.使用串联四级杆EI离子源离子扫描,多反应监测(MRM)模式检测定性.结果... 
Journal Article
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