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Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2012, Volume 68, Issue 12, pp. m1444 - M1444
In the title iron(II) complex, [Fe(C12H21N2Si)Cl(C6H16N2)], the Fe II cation is coordinated by two N atoms from the tetramethylethane-1,2-diamine ligand [Fe-N... 
R factor = 0.060 | mean ω(C-C) = 0.010 Å | single-crystal X-ray study | T = 293 K | wR factor = 0.190 | data-to-parameter ratio = 18.7 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 08/2012, Volume 68, Issue 8, pp. o2405 - o2406
In the title compound, C28H21ClN4O4, the benzofuran ring systems make dihedral angles of 7.43 (8) and 30.92 (9)degrees with the chloro-substituted benzene... 
data-to-parameter ratio = 19.9 | wR factor = 0.144 | single-crystal X-ray study | mean σ(C-C) = 0.003 Å | R factor = 0.048 | T = 100 K | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 08/2011, Volume 67, Issue 8, pp. m1027 - U291
The asymmetric unit of the title compound, [ZnCl2(C11H17N3)], contains two independent pentacoordinate Zn-II complex molecules. In each molecule, the metal... 
mean σ(CC) = 0.003 Å | single-crystal X-ray study | wR factor = 0.052 | R factor = 0.021 | data-to-parameter ratio = 20.1 | T = 100 K | CRYSTAL | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 03/2012, Volume 68, Issue 3, pp. m296 - U716
In the title compound, [Ge(C(9)H(11)O)(2)(C(6)H(16)N(2))], the Ge(II) atom is coordinated in a distorted trigonal-pyramidal geometry by two O atoms belonging... 
wR factor = 0.082 | single-crystal X-ray study | mean σ(C-C) = 0.003 Å | T = 173 K | data-to-parameter ratio = 19.6 | R factor = 0.030 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 08/2012, Volume 68, Issue 8, pp. m1129 - M1129
In the title complex, cis-[PdI2(C6H16N2)], the Pd II atom lies on a crystallographic twofold rotation axis and is four-coordinated by the two N atoms of a... 
wR factor = 0.060 | data-to-parameter ratio = 25.5 | single-crystal X-ray study | R factor = 0.023 | mean σ(C-C) = 0.006 Å | T = 100 K | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2012, Volume 68, Issue 12, pp. m1474 - M1474
In the heterometallic title bulky amido complex, [LiNa(C15H21N2Si)(2)(C6H16N2)], both alkali metal ions are four-coordinated with distorted tetrahedral... 
data-to-parameter ratio = 19.1 | mean ω(C-C) = 0.007 Å | single-crystal X-ray study | wR factor = 0.195 | T = 295 K | R factor = 0.062 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 02/2013, Volume 69, Issue 2, pp. m117 - m118
In the title compound, cis-[PtCl2(C5H13N3)(C2H6OS)], the four-coordinate Pt II atom is bonded to one N atom of the N, N, N',N'-tetramethylguanidine ligand, one... 
T = 120 K | wR factor = 0.045 | data-to-parameter ratio = 23.1 | single-crystal X-ray study | R factor = 0.023 | mean σ(N-C) = 0.007 Å | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 2014, Volume 70, Issue 5, pp. m179 - M179
In the title compound, [Pd(CF3)(C6H4F)(C6H16N2)], the Pd II cation is four- coordinated by the two N atoms of the N, N, N', N'-tetramethylethylenediamine... 
wR factor = 0.067 | mean σ(C-C) = 0.005 A | single-crystal X-ray study | data-to-parameter ratio = 16.0 | R factor = 0.026 | T = 296 K | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2012, Volume 68, Issue 12, pp. m1562 - M1562
In the title complex, [PtCl2(C6H16N2)], the Pt II atom adopts a distorted cis-PtN2Cl2 square-planar coordination geometry. The five-membered chelate ring... 
data-to-parameter ratio = 19.9 | mean ω(C-C) = 0.010 Å | R factor = 0.044 | single-crystal X-ray study | wR factor = 0.116 | T = 296 K | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2012, Volume 68, Issue 12, pp. m1568 - m1569
In the title compound, [Fe(C9H13N4O4)(NH3)(2)], the Fe III atom, lying on a mirror plane, is coordinated by four N atoms of a triply deprotonated tetradentate... 
single-crystal X-ray study | mean ω(C-C) = 0.004 Å | T = 100 K | data-to-parameter ratio = 12.9 | wR factor = 0.074 | disorder in main residue | R factor = 0.030 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 11/2012, Volume 68, Issue 11, pp. m1398 - m1399
The title complex, [Co(C10H9N4O2S)(2)(C3H7NO)(2)], lies across an inversion center. The Co-II atom is coordinated in a slightly distorted octahedral geometry... 
mean ̄(C-C) = 0.004 Å | T = 298 K | single-crystal X-ray study | wR factor = 0.095 | data-to-parameter ratio = 15.7 | R factor = 0.040 | disorder in main residue | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 02/2013, Volume 69, Issue 2, pp. m121 - m121
In the title monomeric rare earth complex, [LiNd(C(19)H(40)N(3)Si(2))(2)Cl(2)(C(4)H(8)O)(2)], the [(Me(3)Si)(2)NC(NCy)(2)](2)Nd(+) (Me is methyl, Cy is... 
mean σ(C-C) = 0.008 Å | wR factor = 0.111 | single-crystal X-ray study | T = 223 K | R factor = 0.051 | data-to-parameter ratio = 20.0
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 01/2012, Volume 68, Issue 1, pp. m64 - M64
In the title compound, [FeCl2(C34H36N4)], the Fe-II ion is coordinated by two Cl atoms and by two N atoms from a (1R,2R)-N,N... 
T = 298 K | wR factor = 0.093 | Data-to-parameter ratio = 21.8 | Mean σ(C-C) = 0.004 Å | R factor = 0.037 | Single-crystal X-ray study | CRYSTALLOGRAPHY | HYDROGENATION | COMPLEXES
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 02/2012, Volume 68, Issue 2, pp. m202 - U1099
The asymmetric unit of the title compound, [Zn(NCS)(C12H7ClN2)(2)][Zn(NCS)(3)(C12H7ClN2)], contains two cations and two anions. In the cations, the Zn-II ions... 
R factor = 0.072 | T = 298 K | mean σ(C-C) = 0.013 Å | single-crystal X-ray study | data-to-parameter ratio = 16.0 | wR factor = 0.250 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 02/2013, Volume 69, Issue 2, pp. o292 - O292
In the crystal structure of the title salt, C12H30N42+center dot 2C(24)H(20)B(-), the C-N bond lengths in the central CN3 unit of the guanidinium ion are... 
wR factor = 0.108 | mean σ(C-C) = 0.002 Å | single-crystal X-ray study | R factor = 0.045 | T = 100 K | data-to-parameter ratio = 20.0 | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2011, Volume 67, Issue 12, pp. o3425 - o3426
The P atom in the title molecule, C24H28N3O2P, is in a distorted tetrahedral P(=O)(N)(N)(2) environment. The phosphoryl group and the NH unit adopt a syn... 
T = 120 K | single-crystal X-ray study | mean σ(C-C) = 0.006 Å | wR factor = 0.216 | data-to-parameter ratio = 14.8 | R factor = 0.073 | disorder in main residue | PHOSPHORIC TRIAMIDES | CRYSTALLOGRAPHY | SKELETON
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 03/2012, Volume 68, Issue 3, pp. m273 - m274
The title complex, [Cd(C(6)H(17)N(3))(2)](ClO(4))(NO(3)), was synthesized by the reaction of Cd(NO(3))(2)·4H(2)O, bis-(3-amino-prop-yl)-amine and sodium... 
T = 120 K | single-crystal X-ray study | data-to-parameter ratio = 12.7 | wR factor = 0.068 | R factor = 0.022 | mean σ(C-C) = 0.003 Å | disorder in main residue | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 1600-5368, 12/2011, Volume 67, Issue 12, pp. m1854 - m1855
In the title compound, [Pb(NO3)(C38H38N10)][Pb(C38H38N10)-(H2O)(0.5)](NO3)(3)center dot 2H(2)O, both Pb-II ions are coordinated in a distorted... 
T = 298 K | single-crystal X-ray study | wR factor = 0.101 | data-to-parameter ratio = 14.8 | R factor = 0.045 | disorder in main residue | mean σ(C-C) = 0.010 Å | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 2014, Volume 70, Issue 5, pp. o516 - o517
The C-N bond lengths in the guanidine unit of the title compound, C16H18N4O2, are 1.298 (2), 1.353 (2) and 1.401 (3) angstrom, indicating double-and... 
wR factor = 0.124 | single-crystal X-ray study | data-to-parameter ratio = 14.7 | T = 293 K | R factor = 0.053 | mean σ(C-C) = 0.003 A | CRYSTALLOGRAPHY
Journal Article
Acta Crystallographica Section E: Structure Reports Online, ISSN 2056-9890, 08/2011, Volume 67, Issue 8, pp. m1025 - m1026
The asymmetric unit of the title compound, [Co(NCS)(2)(C6H17N3)], consists of one Co2+ cation, two thiocyanate anions and one bis(3-aminopropyl) amine ligand,... 
wR factor = 0.070 | mean σ(CC) = 0.003 Å | data-to-parameter ratio = 22.2 | single-crystal X-ray study | T = 170 K | R factor = 0.027 | CRYSTAL | CRYSTALLOGRAPHY
Journal Article
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